A novel receptor based on a C3v-symmetrical PN3-calix[6]cryptand.
Identifieur interne : 000D65 ( France/Analysis ); précédent : 000D64; suivant : 000D66A novel receptor based on a C3v-symmetrical PN3-calix[6]cryptand.
Auteurs : Xianshun Zeng [France] ; Nicolas Hucher ; Olivia Reinaud ; Ivan JabinSource :
- The Journal of organic chemistry [ 0022-3263 ] ; 2004.
Abstract
A C3v-symmetrical PN3-calix[6]cryptand was prepared in six steps from the known 1,3,5-tris-methylated calix[6]arene through a remarkably efficient [1 + 1] macrocyclization reaction. A 1H NMR study showed that the P,N-crypto cap rigidifies the whole edifice in a cone conformation ideal for molecular recognition applications. The ability of this new receptor to perform selective endo-complexation is illustrated with ammonium guests.
DOI: 10.1021/jo048814b
PubMed: 15387616
Affiliations:
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pubmed:15387616Le document en format XML
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<front><div type="abstract" xml:lang="en">A C3v-symmetrical PN3-calix[6]cryptand was prepared in six steps from the known 1,3,5-tris-methylated calix[6]arene through a remarkably efficient [1 + 1] macrocyclization reaction. A 1H NMR study showed that the P,N-crypto cap rigidifies the whole edifice in a cone conformation ideal for molecular recognition applications. The ability of this new receptor to perform selective endo-complexation is illustrated with ammonium guests.</div>
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